DRAFT: This module has unpublished changes.

Data Analysis

 

Table 1: Test Observations and Results with Known Anions

Procedure Anion Actions Observations Proposed Equations
1. Ba(NO3)2 test (PO4)3- Added Ba(NO3)2 precipitate 3Ba(NO3)2 (aq) + 2PO4 (aq) -> (Ba3)(PO4)2 (s) + 6NO3 (aq)
1. Ba(NO3)2 test (PO4)3- Added HNO3 precipitate dissolved 2HNO3 (aq) + (Ba3)(PO4)2 (s) -> H2PO4 (aq) + Ba(NO3)2 (aq)
1. Ba(NO3)2 test (SO4)2- Added Ba(NO3)2 precipitate  Ba(NO3)2 (aq) + SO4 -> BaSO4 (s) + 2NO3 (aq)
1. Ba(NO3)2 test (SO4)2- Added HNO3 precipitate did not dissolve  HNO3 (aq) + BaSO4 (s) -> Ba(NO3)2 (s) + H2SO4 (aq)
1. Ba(NO3)2 test Cl- Added Ba(NO3)2 no precipitate Ba(NO3)2 (aq) + Cl (aq) -> BaCl (aq) + 2NO3 (aq)
1. Ba(NO3) test (NO3)- Added Ba(NO3)2 no precipitate

Ba(NO3)2 (aq) + NO3 (aq) ->  Ba(NO3)2 (aq) + NO3 (aq)

 2. AgNO3 test  PO4  Added AgNO3  no precipitate

 3AgNO3 (aq) + PO4 (aq)

 -> Ag3PO4 (aq) + 3NO3 (aq)

 2. AgNO3 test  SO4  Added AgNO3  no precipitate

 2AgNO3 (aq) + SO4 (aq)

-> Ag2SO4 (aq) + 2NO3 (aq)

 2. AgNO3 test  Cl Added AgNO3  precipitate

 AgNO3 (aq) + Cl (aq)

->  AgCl (s) + NO3

 2. AgNO3 test  Cl  Added NH3  precipitate dissolved  AgCl (s) + 2NH3 (aq) -> Ag(NH3)2 (aq) + Cl (aq)
 2. AgNO3 test  NO3  Added AgNO3  no precipitate  AgNO3 (aq) + NO3 (aq) -> AgNO3 (aq) + NO3 (aq)
 3. Brown ring test NO3  NO3  Added H2SO4  very faint brown line  H2SO4 (aq) + 2NO3 (aq) -> 2HNO3 (aq) + SO4 (aq)

Table 2:  Analysis of Unknown Solution

Step Action Observations Anion Present
1 Added Ba(NO3)2 no precipitate in unknown Cl-, (NO3)-
2 Added HNO3 no precipitate Cl-, (NO3)-
3 Added AgNO3 precipitate formed Cl-
4 Added H2SO4 no brown ring Cl-, no (NO3)-

Conclusion

 The purpose of this lab was to identify the anions present in the mixture of solution. This was done by using qualitative analysis where different reagents are added to the unknown to determine what the unknown is. When it the result of different reactions are known, this is how the unknown can be determined. The results from this experiment stated that the chloride anion was present in the solution which was accurate. To improve this lab, the experimenters need to make sure that no contamination of chemicals occurs during the procedure. The contamination of chemicals could alter a reaction significantly which could make a precipitate when there should not be one or not have one when there should be. This happened once where there was not a precipitate when we should have had one. When it tested again, a precipitate was formed.

DRAFT: This module has unpublished changes.