DRAFT: This module has unpublished changes.

Set-Up of the Data Collection System:

 

1. Start a new experiment on the data collection system.

 

2. Connect a pH sensor and the Rotary Motion sensor to data collection system.

 

3. In DataStudio create a calculated dataset for Volume.

  

4. In DataStudio create a calculated dataset for the first derivative of the pH vs. Volume. 5. Display the pH on y-axis and Volume on x-axis.

 

6. Setup the Titrator pump.

 

7. Rinse the syringe on the Titrator pump.

 

8. Setup the Titrator Accessory.

 

9. Calibrate the pH sensor.

 

10. Add the micro stir bar to the end of the pH sensor.

 

11. Setup the titrant container and replace the cap on the bottle, but not airtight.

 

12. Load the syringe on the pump with the titrant solution.

 

13. Prime the pump on the Titrator. 

 

14. Mount the jar with the sample on the titration accessory.

DRAFT: This module has unpublished changes.