DRAFT: This module has unpublished changes.

Equipment:

  • Data Collection System
  • Conductivity Sensor
  • Magnetic Stirrer
  • Ring Stand
  • Clamp
  • Beaker (2), 100-mL
  • Beaker, 50-mL
  • Hot Plate/Magnetic Plate
  • Automatic Titrator
  • Jar with custom-made hockey puck-derived lid, 180-mL
  • Hydrochloric Acid, unknown concentration (approximately 6M), 70 mL
  • 0.0200 M Sulfuric Acid, 50-mL
  • Barium Hydroxide, Unknown Concentration, 50-mL
  • Water, deionized, 50 mL
  • Volumetric Pipet, 50-mL
  • Wash Bottle
  • Tissue

 

Method:

  • Gathered all equipment and materials. Inspected all equipment for damage or contamination.
  • Set up Data Collection System, assembled GLX, and conductivity sensor.
  • Set up Automatic Titrator, ring stand, Hot Plate/Magnetic Plate, and attached the Jar with custom-made hockey puck-derived lid.
  • Placed the conductivity sensor so that it would be suspended in the jar, and attached the magnetic stirrer to the end of the sensor.
  • Flushed Automatic Titrator with deionized water, to minimize contamination, before filling with 50 mL of 0.0200 M Sulfuric Acid.
  • Acquired 50 mL of Barium Hydroxide, and poured into Jar.
  • Added deionized water until the solution covered the tip of the conductivity sensor.
  • Turned on Magnetic Stirrer, checked all connections to ensure that they were secure, checked the Automatic Titrator to ensure that no bubbles were present within it, then began titrating.
  • Recorded the Data via the GLX, generating the graphs used.
  • Disposed of solutions in designated containers. Cleaned all glassware, set them to dry in their designated areas, and returned all equipment to its point of origin.
DRAFT: This module has unpublished changes.